(1'S^*,10'S^*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion

Base Information

• Chemical Name: (1'S^*,10'S^*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion
• CAS No.: 100084-60-4
• Molecular Formula: C₁₈H₁₉N₃O₃
• Molecular Weight: 325.367

Synonyms:

Chemical Property of (1'S^*,10'S^*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion

Chemical Property:

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Technology Process of (1'S^*,10'S^*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion

There total 1 articles about (1'S^*,10'S^*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) → (1'S*,10'S*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion (100084-60-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / benzene / 2 h / Heating

2: 38 percent / t-BuOK / dimethylsulfoxide / 0.5 h / Ambient temperature

With potassium tert-butylate; In dimethyl sulfoxide; benzene;

Reference yield: 33.0%

(1'S*,10'S*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion (100084-60-4) → (1S*,10S*)-10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (100164-18-9)

Guidance literature:

With lithium triethylborohydride; In tetrahydrofuran; for 0.2h; Ambient temperature;

Reference yield:

(1'S*,10'S*)-1',11',11'-Trimethyl-4'-phenyl-2',4',6'-triazaspiro2,6>undec<8>en>-3',5'-dion (100084-60-4) → 1,11,11-Trimethyl-10-methylen-4-phenyl-2,4,6-triazatricyclo<5.3.1.02,6>undec-8-en-3,5-dion (100102-77-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 33 percent / lithium triethylhydroborate / tetrahydrofuran / 0.2 h / Ambient temperature

2: POCl₃ / pyridine / 4 h / Heating

With lithium triethylborohydride; trichlorophosphate; In tetrahydrofuran; pyridine;

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

Downstream raw materials:

(1S^*,10S^*)-10-Hydroxy-1,10,11,11-tetramethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

1,11,11-Trimethyl-10-methylen-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

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