C₁₄H₂₀O

Base Information

• Chemical Name: C₁₄H₂₀O
• CAS No.: 1298088-90-0
• Molecular Formula: C₁₄H₂₀O
• Molecular Weight: 204.312
• Mol file: 1298088-90-0.mol

Synonyms:

Chemical Property of C₁₄H₂₀O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀O

There total 2 articles about C₁₄H₂₀O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H20O (1298088-84-2) → C14H20O (1298088-89-7) + C14H20O (1298088-90-0) + (2R)-2-methyl-2-phenylheptanal + (2S)-2-methyl-2-phenylheptanal (570368-32-0)

Guidance literature:

With tetrachlorosilane; 1,3-bis(3,5-bis(trifluoro-ethyl)phenyl)thiourea; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 18h; optical yield given as %ee; Inert atmosphere;

DOI:10.1021/ja110685k

Reference yield:

2-phenyl-2-(E/Z)-octene (53109-16-3,53109-17-4,14673-22-4) → C14H20O (1298088-89-7) + C14H20O (1298088-90-0) + (2R)-2-methyl-2-phenylheptanal + (2S)-2-methyl-2-phenylheptanal (570368-32-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Oxone; Shi's ketone; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate / water; acetonitrile / 0 °C / Inert atmosphere

2: tetrachlorosilane; 1,3-bis(3,5-bis(trifluoro-ethyl)phenyl)thiourea; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

With Oxone; Shi's ketone; tetrachlorosilane; 1,3-bis(3,5-bis(trifluoro-ethyl)phenyl)thiourea; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; acetonitrile;

DOI:10.1021/ja110685k

upstream raw materials:

C₁₄H₂₀O

2-phenyl-2-(E/Z)-octene