1H-Pyrrole-3-carboxamide, N-[3-[[2-[(2,6-dimethylphenyl)amino]-1-methyl-2-oxoethyl]amino]propyl]- 2,5-dihydro-2,2,5,5-tetramethyl-

Base Information

Chemical Name:1H-Pyrrole-3-carboxamide, N-[3-[[2-[(2,6-dimethylphenyl)amino]-1-methyl-2-oxoethyl]amino]propyl]- 2,5-dihydro-2,2,5,5-tetramethyl-
CAS No.:102132-20-7
Molecular Formula:C23H36N4O2
Molecular Weight:400.564
Hs Code.:
Mol file:102132-20-7.mol

Synonyms:

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Chemical Property of 1H-Pyrrole-3-carboxamide, N-[3-[[2-[(2,6-dimethylphenyl)amino]-1-methyl-2-oxoethyl]amino]propyl]- 2,5-dihydro-2,2,5,5-tetramethyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1H-Pyrrole-3-carboxamide, N-[3-[[2-[(2,6-dimethylphenyl)amino]-1-methyl-2-oxoethyl]amino]propyl]- 2,5-dihydro-2,2,5,5-tetramethyl-

There total 2 articles about 1H-Pyrrole-3-carboxamide, N-[3-[[2-[(2,6-dimethylphenyl)amino]-1-methyl-2-oxoethyl]amino]propyl]- 2,5-dihydro-2,2,5,5-tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93799-49-6
2,2,5,5-Tetramethyl-2,5-dihydro-1H-pyrrole-3-carboxylic acid (3-amino-propyl)-amide

: 102132-20-7
2,2,5,5-Tetramethyl-2,5-dihydro-1H-pyrrole-3-carboxylic acid {3-[1-(2,6-dimethyl-phenylcarbamoyl)-ethylamino]-propyl}-amide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 3h;
DOI:10.1021/jm00157a005

Reference yield:

: 19971-12-1
3,5-Dibromo-4-oxo-2,2,6,6-tetramethylpiperidine Hydrobromide

: 102132-20-7
2,2,5,5-Tetramethyl-2,5-dihydro-1H-pyrrole-3-carboxylic acid {3-[1-(2,6-dimethyl-phenylcarbamoyl)-ethylamino]-propyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / H₂O / 3 h / 25 °C

2: K₂CO₃ / dimethylformamide / 3 h / 60 °C

With potassium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00157a005