O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid

Base Information

Chemical Name:O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid
CAS No.:75347-80-7
Molecular Formula:C₆₇H₆₅BrN₄O₂₀
Molecular Weight:1326.17
Hs Code.:

O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid

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Chemical Property of O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid

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Technology Process of O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid

There total 10 articles about O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 75347-79-4
O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranose

: 75347-80-7
O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid

Guidance literature:: With titanium(IV) bromide;

Reference yield:

: 75347-77-2
6-O-acetyl-3-O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-4-O-benzyl-2-desoxy-2-phthalimido-D-galactopyranosylbromide

: 75347-80-7
O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / silver-triflate/collidine

2: 98 percent / trifluoroacetic acid

3: 92 percent / TiBr₄

With 2,3,5-trimethyl-pyridine; silver trifluoromethanesulfonate; titanium(IV) bromide; In trifluoroacetic acid;

Reference yield:

: 75347-76-1
1,6-di-O-acetyl-3-O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranose

: 75347-80-7
O-(6-O-acetyl-2-azido-3,4-di-O-benzoyl-2-desoxy-α-D-galactopyranosyl)-(1->3)-O-(6-O-acetyl-4-O-benzyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1->3)-1,6-di-O-acetyl-2,4-di-O-benzyl-α-D-galactopyranosylbromid

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / TiBr₄

2: 68 percent / silver-triflate/collidine

3: 98 percent / trifluoroacetic acid

4: 92 percent / TiBr₄

With 2,3,5-trimethyl-pyridine; silver trifluoromethanesulfonate; titanium(IV) bromide; In trifluoroacetic acid;