C₁₃H₁₉N₃

Base Information

• Chemical Name: C₁₃H₁₉N₃
• CAS No.: 1035160-79-2
• Molecular Formula: C₁₃H₁₉N₃
• Molecular Weight: 217.314
• Mol file: 1035160-79-2.mol

Synonyms:

Chemical Property of C₁₃H₁₉N₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₃H₁₉N₃

There total 1 articles about C₁₃H₁₉N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

3,5-bis[(dimethylamino)methyl]benzaldehyde (214339-79-4) → C13H19N3 (1035160-79-2)

Guidance literature:

With formic acid; hydroxylamine hydrochloride; for 1.5h; Heating;

DOI:10.1016/j.jorganchem.2008.02.027

Reference yield:

C13H19N3 (1035160-79-2) + tert.-butyl lithium (594-19-4) → C17H28N2O (1035160-72-5) + C17H28(2)HN3 (1035160-70-3)

Guidance literature:

C₁₃H₁₉N₃; tert.-butyl lithium; In diethyl ether; hexane; for 0.5h;

With water-d2; In diethyl ether; hexane; Further stages.;

DOI:10.1016/j.jorganchem.2008.02.027

upstream raw materials:

3,5-bis[(dimethylamino)methyl]benzaldehyde

Downstream raw materials:

C₁₇H₂₈N₂O

C₁₇H₂₈⁽²⁾HN₃