Desfluoro Iloperidone (IMpurity)

Base Information

• Chemical Name: Desfluoro Iloperidone (IMpurity)
• CAS No.: 133454-46-3
• Molecular Formula: C₂₄H₂₈N₂O₄
• Molecular Weight: 408.497
• Mol file: 133454-46-3.mol

Synonyms:

Chemical Property of Desfluoro Iloperidone (IMpurity)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

DesfluoroIloperidone(Impurity) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Desfluoro Iloperidone is the analog of Iloperidone (I267200), with potential application as an anti-psychotic due to the anti-psychotic profile of Iloperidone (I267200). Iloperidone (I267200) is noted for treatment of patients with psychological disorders, primarily schizophrenia in adults. An impurity in the synthesis of Iloperidone (I267200).

Technology Process of Desfluoro Iloperidone (IMpurity)

There total 4 articles about Desfluoro Iloperidone (IMpurity) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(3-chloropropoxy)-3-methoxyacetophenone (58113-30-7) + potassium carbonate (584-08-7) + 3-(4-piperidinyl)-1,2-benzisoxazole hydrochloride (84163-22-4) → 1-[4-[3-[4-(1,2-benzisoxazol-3-yl)-1-piperidinyl]propoxy]-3-methoxyphenyl]ethanone (133454-46-3)

Guidance literature:

With Ki; In N-methyl-acetamide;

Reference yield:

4-(3-chloropropoxy)-3-methoxyacetophenone (58113-30-7) + 3-(4-piperidinyl)-1,2-benzisoxazole hydrochloride (84163-22-4) → 1-[4-[3-[4-(1,2-benzisoxazol-3-yl)-1-piperidinyl]propoxy]-3-methoxyphenyl]ethanone (133454-46-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 16h;

DOI:10.1021/jm00007a009

Reference yield:

1-[4-(3-chloropropoxy)-3-methoxyphenyl]ethamone + potassium carbonate (584-08-7) + 3-(4-piperidinyl)-1,2-benzisoxazole hydrochloride (84163-22-4) → 1-[4-[3-[4-(1,2-Benzisoxazol-3-yl)-1-piperidinyl]propoxy]-3-methoyphenyl]-ethanane + 1-[4-[3-[4-(1,2-benzisoxazol-3-yl)-1-piperidinyl]propoxy]-3-methoxyphenyl]ethanone (133454-46-3)

Guidance literature:

upstream raw materials:

4-(3-chloropropoxy)-3-methoxyacetophenone

3-(4-piperidinyl)-1,2-benzisoxazole hydrochloride

potassium carbonate

1-(3-methoxy-4-hydroxyphenyl)ethanone

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