[Co(3,5-dimethylpyrazole)2(benzoato)2]

Base Information

Chemical Name:[Co(3,5-dimethylpyrazole)2(benzoato)2]
CAS No.:1297274-88-4
Molecular Formula:C₂₄H₂₆CoN₄O₄
Molecular Weight:493.488
Hs Code.:

Synonyms:

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Chemical Property of [Co(3,5-dimethylpyrazole)2(benzoato)2]

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Technology Process of [Co(3,5-dimethylpyrazole)2(benzoato)2]

There total 2 articles about [Co(3,5-dimethylpyrazole)2(benzoato)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.8%

: 67-51-6
3,5-dimethyl-1H-pyrazole

: Co3(μ-benzoato)4(μ,η2-benzoato)2[OC(Ph)OHNEt3]2

: 1297274-88-4
[Co(3,5-dimethylpyrazole)2(benzoato)2]

Guidance literature:: In benzene; (Ar): addn. soln. of 3,5-dimethylpyrazole in benzene to soln. of Co3(.mu-OOCPh)4(μ,η2-OOCPh)2(OC(Ph)OHNEt3)2 in benzene at 22°C; concn., cooling at 5°C for 2 ds, crystn., decantation, washing with cold hexane, drying in Ar flow; elem. anal.;
DOI:10.1134/S0036023610070119

Reference yield: 71.0%

: 615251-39-3
bis(3,5-dimethylpyrazole)bis(trimethylacetato)bis(μ-N,N'-3,5-dimethylpyrazolato)dicobalt(II)

: 65-85-0,8013-63-6
benzoic acid

: 1297274-88-4
[Co(3,5-dimethylpyrazole)2(benzoato)2]

Guidance literature:: In o-xylene; (Ar); addn. of benzoic acid to soln. of Co2(μ-3,5-dimethylpyrazolato)2(3,5-dimethylpyrazole)2(pivalato)2 in o-xylene, stirring at 140°C for 3 h; concn., cooling at 5°C for sevaral days, crystn., decantation, washing with cold hexane, drying in Ar flow;
DOI:10.1134/S0036023610070119

Reference yield: 52.0%

: 1297274-88-4
[Co(3,5-dimethylpyrazole)2(benzoato)2]

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 1297293-98-1
Co2(μ-3,5-dimethylpyrazole(-1H))2(3,5-dimethylpyrazole)2(benzoate)2

Guidance literature:: In o-xylene; under Ar atm.; to soln. of Co complex in o-xylene, Co acetate hydrate was added; mixt. stirred at 140-145°C for 3 h; filtered; kept at 5°C for several ds; crystals sepd. from mother liquor by decantation; washed (hexane); dried in Ar flow; elem. anal.;
DOI:10.1134/S003602361009010X