C₂₉H₄₄N₂O

Base Information

Chemical Name:C₂₉H₄₄N₂O
CAS No.:1295581-16-6
Molecular Formula:C₂₉H₄₄N₂O
Molecular Weight:436.681
Hs Code.:

C<sub>29</sub>H<sub>44</sub>N<sub>2</sub>O

Synonyms:

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Chemical Property of C₂₉H₄₄N₂O

Chemical Property:

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Technology Process of C₂₉H₄₄N₂O

There total 16 articles about C₂₉H₄₄N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57766-63-9,55784-75-3
(3S)-geranyllinaloisocyanide

: 1295581-16-6
C₂₉H₄₄N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine N-oxide; iodine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

2: acetonitrile / 1 h / 20 °C / Inert atmosphere

With pyridine N-oxide; iodine; In acetonitrile;
DOI:10.1021/ol200308m

Reference yield:

: 1295581-02-0
(S,E)-tert-butyl 4-(3-ethoxy-3-oxoprop-1-enyl)-2,2,4-trimethyloxazolidine-3-carboxylate

: 1295581-16-6
C₂₉H₄₄N₂O

Guidance literature:: Multi-step reaction with 16 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.58 h / -78 °C / Inert atmosphere

3.1: dichloromethane / 84 h / 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.58 h / -78 °C / Inert atmosphere

5.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

6.1: lithium bromide / tetrahydrofuran / 1 h / -10 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 - -10 °C / Inert atmosphere

7.2: 0.33 h / -10 - 20 °C / Inert atmosphere

8.1: dichloro [1,1'-bis(diphenylphosphino)propane]palladium(II); lithium triethylborohydride / tetrahydrofuran / 7.5 h / 0 °C / Inert atmosphere

9.1: water; scandium tris(trifluoromethanesulfonate) / acetonitrile / 74 h / 20 °C

10.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 9 h / 20 °C / Inert atmosphere

11.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 - 20 °C / Inert atmosphere

12.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran; toluene / 0.17 h / 20 °C / Inert atmosphere

13.1: sodium hydrogencarbonate / dichloromethane; water / 4 h / 20 °C

14.1: carbon tetrabromide; triethylamine; triphenylphosphine / dichloromethane / 0.25 h / -10 - 20 °C / Inert atmosphere

15.1: pyridine N-oxide; iodine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

16.1: acetonitrile / 1 h / 20 °C / Inert atmosphere

With pyridine N-oxide; 2,6-dimethylpyridine; n-butyllithium; dichloro [1,1'-bis(diphenylphosphino)propane]palladium(II); carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; water; hydrogen; iodine; potassium hexamethylsilazane; diisobutylaluminium hydride; lithium triethylborohydride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; lithium bromide; scandium tris(trifluoromethanesulfonate); 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; 3.1: Wittig reaction / 11.1: Wittig reaction;
DOI:10.1021/ol200308m

Reference yield:

: 1295581-18-8
(S)-tert-butyl 4-(3-ethoxy-3-oxopropyl)-2,2,4-trimethyloxazolidine-3-carboxylate

: 1295581-16-6
C₂₉H₄₄N₂O

Guidance literature:: Multi-step reaction with 15 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.58 h / -78 °C / Inert atmosphere

2.1: dichloromethane / 84 h / 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.58 h / -78 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

5.1: lithium bromide / tetrahydrofuran / 1 h / -10 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 - -10 °C / Inert atmosphere

6.2: 0.33 h / -10 - 20 °C / Inert atmosphere

7.1: dichloro [1,1'-bis(diphenylphosphino)propane]palladium(II); lithium triethylborohydride / tetrahydrofuran / 7.5 h / 0 °C / Inert atmosphere

8.1: water; scandium tris(trifluoromethanesulfonate) / acetonitrile / 74 h / 20 °C

9.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 9 h / 20 °C / Inert atmosphere

10.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 - 20 °C / Inert atmosphere

11.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran; toluene / 0.17 h / 20 °C / Inert atmosphere

12.1: sodium hydrogencarbonate / dichloromethane; water / 4 h / 20 °C

13.1: carbon tetrabromide; triethylamine; triphenylphosphine / dichloromethane / 0.25 h / -10 - 20 °C / Inert atmosphere

14.1: pyridine N-oxide; iodine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

15.1: acetonitrile / 1 h / 20 °C / Inert atmosphere

With pyridine N-oxide; 2,6-dimethylpyridine; n-butyllithium; dichloro [1,1'-bis(diphenylphosphino)propane]palladium(II); carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; water; iodine; potassium hexamethylsilazane; diisobutylaluminium hydride; lithium triethylborohydride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; lithium bromide; scandium tris(trifluoromethanesulfonate); 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; 2.1: Wittig reaction / 10.1: Wittig reaction;
DOI:10.1021/ol200308m