methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)

Base Information

Chemical Name:methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)
CAS No.:87256-62-0
Molecular Formula:C₂₈H₃₈N₂O₁₄
Molecular Weight:626.615
Hs Code.:

methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)

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Chemical Property of methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)

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Technology Process of methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)

There total 5 articles about methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26775-14-4
3-O-acetyl-1,2:5,6-di-O-isopropylidene-α-D-gulofuranose

: 87256-62-0
methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / aq. acetic acid

3: 98 percent / NaI

4: 43 percent / sodium nitrile

5: 2.) KF / 2.) acetonitrile

With potassium fluoride; sodium nitrile; acetic acid; sodium iodide;
DOI:10.1246/cl.1983.819

Reference yield:

: 51433-05-7
3'-O-acetyl-1',2'-O-isopropylidene-5',6'-diol-α-D-allofuranose

: 87256-62-0
methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)

Guidance literature:: Multi-step reaction with 4 steps

2: 98 percent / NaI

3: 43 percent / sodium nitrile

4: 2.) KF / 2.) acetonitrile

With potassium fluoride; sodium nitrile; sodium iodide;
DOI:10.1246/cl.1983.819

Reference yield:

: 87256-60-8
Acetic acid (3aR,5S,6S,6aR)-5-iodomethyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

: 87256-62-0
methyl-9-O-acetyl-2-(benzyloxycarbonyl)amino-2,7-dideoxy-3,4:10,11-di-O-isopropylidene-7-nitro-β-L-undecodialdo-(11R)-furanose-(11,8)-pyranoside-(1,5)

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / sodium nitrile

2: 2.) KF / 2.) acetonitrile

With potassium fluoride; sodium nitrile;
DOI:10.1246/cl.1983.819