C₃₄H₃₈N₆O₆

Base Information

• Chemical Name: C₃₄H₃₈N₆O₆
• CAS No.: 1360540-08-4
• Molecular Formula: C₃₄H₃₈N₆O₆
• Molecular Weight: 626.712
• Mol file: 1360540-08-4.mol

Synonyms:

Chemical Property of C₃₄H₃₈N₆O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₈N₆O₆

There total 7 articles about C₃₄H₃₈N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H30N6O4 (1360540-01-7) + 2-bromo-3'-methoxyacetophenone (5000-65-7) → C34H38N6O6 (1360540-08-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1016/j.bmcl.2011.11.054

Reference yield:

C15H14N4O2 → C34H38N6O6 (1360540-08-4)

Guidance literature:

Multi-step reaction with 5 steps

1: bromine; acetic acid / 18 h / 45 °C

2: 4-methyl-morpholine / N,N-dimethyl acetamide / 0.33 h / 160 °C / Microwave irradiation

3: palladium 10% on activated carbon; ammonium formate / 0.5 h / 75 °C

4: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 °C

5: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With 4-methyl-morpholine; palladium 10% on activated carbon; bromine; ammonium formate; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.11.054

Reference yield:

C15H13BrN4O2 → C34H38N6O6 (1360540-08-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 4-methyl-morpholine / N,N-dimethyl acetamide / 0.33 h / 160 °C / Microwave irradiation

2: palladium 10% on activated carbon; ammonium formate / 0.5 h / 75 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 °C

4: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With 4-methyl-morpholine; palladium 10% on activated carbon; ammonium formate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.11.054

upstream raw materials:

C₁₈H₂₄N₆O₄

C₂₅H₃₀N₆O₄

2-bromo-3'-methoxyacetophenone

ethyl 3-amino-1-benzyl-4-cyano-1H-pyrrole-2-carboxylate