Ru(C₆H₅NC(CH₃)C(CH₃)NC₆H₅)2Cl₂

Base Information

Chemical Name:Ru(C₆H₅NC(CH₃)C(CH₃)NC₆H₅)2Cl₂
CAS No.:90742-37-3
Molecular Formula:C₃₂H₃₂Cl₂N₄Ru
Molecular Weight:644.609
Hs Code.:

Ru(C<sub>6</sub>H<sub>5</sub>NC(CH<sub>3</sub>)C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>5</sub>)2Cl<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ru(C₆H₅NC(CH₃)C(CH₃)NC₆H₅)2Cl₂

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Technology Process of Ru(C₆H₅NC(CH₃)C(CH₃)NC₆H₅)2Cl₂

There total 1 articles about Ru(C₆H₅NC(CH₃)C(CH₃)NC₆H₅)2Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 2,3-dimethyl-1,4-diphenyl-1,4-diazabuta-1,3-diene

: 21503-87-7,51014-03-0
trans-{RuCl₂(C₆H₅CN)4}

: 90742-37-3
Ru(C₆H₅NC(CH₃)C(CH₃)NC₆H₅)2Cl₂

: 90821-16-2
Ru(C₆H₅NC(CH₃)C(CH₃)NC₆H₅)2Cl₂

Guidance literature:: In diethylene glycol; heating Ru-complex in the presence of excess ligand to the boiling point of diglyme within a period of 30 min (N2-atmosphere); boiling for further 5 min; cooling; crystn. of trans complex within 3 days at -20°C; filtration; washing (acetone); drying in vac.; refluxing mother liquid for 3h; removingsolvent; extg. ligand with petroleum ether; crystn. of cis complex (CH2Cl2/petroleum ether); elem. anal.;