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Technology Process of Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6

Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6

Base Information
  • Chemical Name:Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6
  • CAS No.:133793-82-5
  • Molecular Formula:C33H30ClN6Os*F6P
  • Molecular Weight:881.259
  • Hs Code.:
Os(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2((C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)(CH<sub>2</sub>)3)Cl<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[Os(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2((C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)(CH<sub>2</sub>)3)Cl]PF<sub>6</sub>

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Chemical Property of Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6
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Technology Process of Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6

There total 1 articles about Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(2,2'-bipyridine)osmium(II) dichloride
15702-72-4,79982-56-2

bis(2,2'-bipyridine)osmium(II) dichloride

1,3-di(4-pyridyl)propane
17252-51-6

1,3-di(4-pyridyl)propane

Os(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2((C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)(CH<sub>2</sub>)3)Cl<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[Os(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2((C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)(CH<sub>2</sub>)3)Cl]PF<sub>6</sub>
133793-82-5,155888-48-5,136655-29-3

Os(C10H8N2)2((C10H8N2)(CH2)3)Cl(1+)*PF6(1-)=[Os(C10H8N2)2((C10H8N2)(CH2)3)Cl]PF6

Guidance literature:
In ethylene glycol; soln. of Os-compd. was refluxed with 2 equiv. 4,4'-trimethylenedipyridine for 3h under N2; cooled, equiv. water was added, filtd., satd. aq. soln. of NH4PF6 was added, collected, washed with water, dried with ether, cromd. on alumina with 15% MeOH in toluene;
DOI:10.1021/j100176a098
upstream raw materials:

bis(2,2'-bipyridine)osmium(II) dichloride

1,3-di(4-pyridyl)propane

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