(((CH₃)2CH)2C₆H₃O)3Ta(CC(CH₃)3CHCC(CH₃)3CH)

Base Information

• Chemical Name: (((CH₃)2CH)2C₆H₃O)3Ta(CC(CH₃)3CHCC(CH₃)3CH)
• CAS No.: 130220-40-5
• Molecular Formula: C₄₈H₇₁O₃Ta
• Molecular Weight: 877.038
• Mol file: 130220-40-5.mol

Synonyms:

Chemical Property of (((CH₃)2CH)2C₆H₃O)3Ta(CC(CH₃)3CHCC(CH₃)3CH)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (((CH₃)2CH)2C₆H₃O)3Ta(CC(CH₃)3CHCC(CH₃)3CH)

There total 1 articles about (((CH₃)2CH)2C₆H₃O)3Ta(CC(CH₃)3CHCC(CH₃)3CH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

3,3-Dimethylbut-1-yne (917-92-0) + (quinoline)Ta(O-2,6-C6H3i-Pr2)3Cl2(OEt2) (111618-74-7) → (((CH3)2CH)2C6H3O)3Ta(CC(CH3)3CHCC(CH3)3CH) (130220-40-5)

Guidance literature:

With Na#Hg; In diethyl ether; to a -40°C soln. of Ta-compd. is added 3,3-dimethyl-1-butyne and Na#Hg (0.59%), stirred at room temp. for 48 h,; filtn. through Celite, removal of solvent, dissoln. in pentane, storing at -40°C for 48 h, filtn., washing with cold (-30°C) pentane, drying in vacuo, recrystn. from pentane, elem. anal.;

DOI:10.1021/om00047a038

upstream raw materials:

3,3-Dimethylbut-1-yne

(quinoline)Ta(O-2,6-C₆H₃i-Pr₂)3Cl₂(OEt₂)