o-CH₃OC₆H₄-ferrocenylthiosemicarbazone

Base Information

• Chemical Name: o-CH₃OC₆H₄-ferrocenylthiosemicarbazone
• CAS No.: 1009563-69-2
• Molecular Formula: C₁₉H₁₉FeN₃OS
• Molecular Weight: 393.292
• Mol file: 1009563-69-2.mol

Synonyms:

Chemical Property of o-CH₃OC₆H₄-ferrocenylthiosemicarbazone

Chemical Property:

Purity/Quality:

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Technology Process of o-CH₃OC₆H₄-ferrocenylthiosemicarbazone

There total 1 articles about o-CH₃OC₆H₄-ferrocenylthiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ferrocenecarboxaldehyde (12093-10-6) + 4-(o-methoxyphenyl)thiosemicarbazide (40207-02-1) → o-CH3OC6H4-ferrocenylthiosemicarbazone (1009563-69-2)

Guidance literature:

With CH₃COOH; In methanol; ferrocenecarboxaldehyde and aromatic thiosemicarbazide refluxed in methanol with CH3COOH for 3 h; soln. cooled at ice-bath; precipitate collected by filtration and washedwith methanol several times; recrystallization from CHCl3/MeOH;

DOI:10.1016/j.inoche.2007.09.015

upstream raw materials:

ferrocenecarboxaldehyde

4-(o-methoxyphenyl)thiosemicarbazide