1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane

Base Information

• Chemical Name: 1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane
• CAS No.: 1384213-49-3
• Molecular Formula: C₃₀H₂₈FeN₂O₃
• Molecular Weight: 520.411
• Mol file: 1384213-49-3.mol

Synonyms:

Chemical Property of 1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane

There total 2 articles about 1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

[3]ferrocenophane-1-one + 4,4'-bis(acetamido)benzophenone (50296-99-6) → C30H28FeN2O2 (1254710-15-0) + 1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane (1384213-49-3)

Guidance literature:

[3]ferrocenophane-1-one; 4,4'-bis(acetamido)benzophenone; With titanium tetrachloride; zinc; In tetrahydrofuran; Schlenk technique; Reflux; Inert atmosphere;

With hydrogenchloride; Schlenk technique; Inert atmosphere;

DOI:10.1021/om300382h

Reference yield: 33.0%

[3]ferrocenophane-1-one + 4,4'-bis(acetamido)benzophenone (50296-99-6) → 1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane (1384213-49-3)

Guidance literature:

[3]ferrocenophane-1-one; 4,4'-bis(acetamido)benzophenone; With titanium tetrachloride; benzene-1,2-diol; zinc; In tetrahydrofuran; for 72h; Inert atmosphere; Schlenk technique; Reflux;

With hydrogenchloride; water; In tetrahydrofuran; Schlenk technique; Inert atmosphere;

DOI:10.1021/om300382h

Reference yield: 32.0%

1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane (1384213-49-3) → 1,1-bis(p-aminophenyl)-2-oxo[4]ferrocenophane (1384213-51-7)

Guidance literature:

1-bis(p-acetamidophenyl)-1-phenyl-2-oxo[4]ferrocenophane; With hydrogenchloride; water; In ethanol; for 72h; Schlenk technique; Inert atmosphere; Reflux;

With sodium hydrogencarbonate; In ethanol; water; Schlenk technique; Inert atmosphere;

DOI:10.1021/om300382h

upstream raw materials:

4,4'-bis(acetamido)benzophenone

Downstream raw materials:

1,1-bis(p-aminophenyl)-2-oxo[4]ferrocenophane

Refernces