5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

Base Information

Chemical Name:5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene
CAS No.:1394291-90-7
Molecular Formula:C₅₂H₄₈B₂F₄N₄
Molecular Weight:826.596
Hs Code.:

5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

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Chemical Property of 5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

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Technology Process of 5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

There total 2 articles about 5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1394291-87-2
5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-1,4,8,10,13,17-hexahydro-1,4:8,17:10,13-triethano-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

: 1394291-90-7
5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

Guidance literature:: at 235 ℃; for 2h;
DOI:10.1039/c2ob25930c

Reference yield:

: 1394290-14-2
1,5-dimethyl-3,7-bis[(3-methyl-4,7-dihydro-4,7-ethano-2H-isoindolyl)(4-tert-butyl-phenyl)methyl]-4,8-dihydro-4,8-ethanopyrrolo[3,4-f]isoindole

: 1394291-90-7
5,9-bis(4-tert-butylphenyl)-6,6,15,15-tetrafluoro-5,7,14,16-tetramethyl-6,15-dibora-5a,6a,14a,15a-tetraaza-s-indaceno[2,3-b:6,7-b′]difluorene

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

2: 2 h / 235 °C

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1039/c2ob25930c