2-(4-(Dihexylamino)benzylidene)malononitrile

Base Information

Chemical Name:2-(4-(Dihexylamino)benzylidene)malononitrile
CAS No.:102348-86-7
Molecular Formula:C₂₂H₃₁N₃
Molecular Weight:337.508
Hs Code.:
DSSTox Substance ID:DTXSID50566681
Nikkaji Number:J3.282.221E
Mol file:102348-86-7.mol

Synonyms:102348-86-7;2-(4-(dihexylamino)benzylidene)malononitrile;{[4-(Dihexylamino)phenyl]methylidene}propanedinitrile;SCHEMBL9772923;DTXSID50566681

Suppliers and Price of 2-(4-(Dihexylamino)benzylidene)malononitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-(Dihexylamino)benzylidene)malononitrile

Chemical Property:

XLogP3:6.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:12
Exact Mass:337.251798002
Heavy Atom Count:25
Complexity:438

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCCCN(CCCCCC)C1=CC=C(C=C1)C=C(C#N)C#N

Technology Process of 2-(4-(Dihexylamino)benzylidene)malononitrile

There total 3 articles about 2-(4-(Dihexylamino)benzylidene)malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 90133-80-5
4-formyl-N,N-dihexylaniline

: 109-77-3
malononitrile

: 102348-86-7
2-(4-(dihexylamino)benzylidene)malononitrile

Guidance literature:: With sodium carbonate; for 1h;
DOI:10.1002/chem.201302874

Reference yield:

: 62-53-3
aniline

: 102348-86-7
2-(4-(dihexylamino)benzylidene)malononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate; potassium iodide / 12 h / 160 °C / Reflux

2: trichlorophosphate / N,N-dimethyl-formamide / 12.5 h / 70 °C / Reflux

3: sodium carbonate / 1 h

With sodium carbonate; potassium iodide; trichlorophosphate; In N,N-dimethyl-formamide; 3: |Knoevenagel Condensation;
DOI:10.1002/chem.201302874

Reference yield:

: 111-25-1
1-bromo-hexane

: 102348-86-7
2-(4-(dihexylamino)benzylidene)malononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate; potassium iodide / 12 h / 160 °C / Reflux

2: trichlorophosphate / N,N-dimethyl-formamide / 12.5 h / 70 °C / Reflux

3: sodium carbonate / 1 h

With sodium carbonate; potassium iodide; trichlorophosphate; In N,N-dimethyl-formamide; 3: |Knoevenagel Condensation;
DOI:10.1002/chem.201302874