Technology Process of C58H51N3S
There total 11 articles about C58H51N3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride;
In
tetrahydrofuran; ethanol;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1002/chem.201100033
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran; ethanol / 8 h / Reflux; Inert atmosphere
2: sodium cyanoborohydride / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere
With
sodium cyanoborohydride;
In
tetrahydrofuran; ethanol;
DOI:10.1002/chem.201100033
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 8 h / Reflux; Inert atmosphere
2: tetrahydrofuran; ethanol / 8 h / Reflux; Inert atmosphere
3: sodium cyanoborohydride / tetrahydrofuran; ethanol / 0.5 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium cyanoborohydride; triethylamine;
In
tetrahydrofuran; ethanol;
DOI:10.1002/chem.201100033