fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

Base Information

Chemical Name:fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆
CAS No.:121241-56-3
Molecular Formula:C₄₇H₄₀FeN₃P₂*F₆P
Molecular Weight:909.613
Hs Code.:

fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF<sub>6</sub>

Synonyms:

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Chemical Property of fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

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Technology Process of fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

There total 2 articles about fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 121241-56-3,121313-40-4
mer-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

: 121241-56-3,121313-40-4
fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

Guidance literature:: In tetrahydrofuran; dry oxygen-free argon atmosphere; refluxed for 10 min, solvent was removed in vacuo, addn. of diethyl ether yield a yellow ppt.; elemental analysis;

Reference yield: 70.0%

: ammonium hexafluorophosphate

: 121241-52-9
{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

: 121241-56-3,121313-40-4
mer-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

Guidance literature:: In toluene; dry oxygen-free argon atmosphere; to a soln. of {Fe(dppe)(CNPh)3} in toluene was added NH4PF6 in deaerated distilled water, stirred for 2 h, yellow ppt. was formed; filtration, washed with three successive portions of water, dried in vacuo; elemental analysis;

Reference yield: 90.0%

: 121241-56-3,121313-40-4
mer-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

: 121241-56-3,121313-40-4
fac-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

Guidance literature:: In tetrahydrofuran; dry oxygen-free argon atmosphere; refluxed for 10 min, solvent was removed in vacuo, addn. of diethyl ether yield a yellow ppt.; elemental analysis;