FRh(C₂F₄)(P(C₆H₅)3)2

Base Information

Chemical Name:FRh(C₂F₄)(P(C₆H₅)3)2
CAS No.:107272-42-4
Molecular Formula:C₃₈H₃₀F₅P₂Rh
Molecular Weight:746.501
Hs Code.:

FRh(C<sub>2</sub>F<sub>4</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of FRh(C₂F₄)(P(C₆H₅)3)2

Chemical Property:

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Technology Process of FRh(C₂F₄)(P(C₆H₅)3)2

There total 2 articles about FRh(C₂F₄)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (FRh(C₂H₄)(C₂F₄))4

: 107272-42-4
FRh(C₂F₄)(P(C₆H₅)3)2

Guidance literature:: With triphenyl phosphine; In dichloromethane; Soln. of complex in CH2Cl2 was treated with PPh3 over 30 min, then soln. was stirred for 14 h at room temp. (N2 atm.);; volume was reduced, ether was added, ppt. was filtered, washed and dried;;
DOI:10.1021/om00148a016

Reference yield:

: 12216-72-7,33009-49-3
ClRh(C₂F₄)(P(C₆H₅)3)2

: 150746-76-2
tris(dimethylamino)sulfonium trimethylsilyldifluoride

: 107272-42-4
FRh(C₂F₄)(P(C₆H₅)3)2

Guidance literature:: With AgBF₄; In tetrahydrofuran; byproducts: AgCl; Soln. of complex and AgBF4 in THF was stirred for 1 h at room temp.; filtered and was treated with 2 equiv of (Me2N)3S(1+)*Me3SiF2(1-); soln. was stirred for 1 h (atm. N2);; cooling to -35°C for 12 h; recrystd. from CH2Cl2/ether/pentane; elem. anal.;;
DOI:10.1021/om00148a016

Reference yield:

: 107272-42-4
FRh(C₂F₄)(P(C₆H₅)3)2

: 58167-05-8,22481-17-0
fluorocarbonylbis(triphenylphosphine)rhodium(I)

Guidance literature:: With CO; In dichloromethane; Soln. of complex in CH2Cl2 was treated with CO;; ether-pentane was added, cooled to -35°C for 24 h;;
DOI:10.1021/om00148a016