di(phenylboron) chelate of 3-amino-5-oxo-5-phenylpent-3-enolhydrazide*benzene

Base Information

Chemical Name:di(phenylboron) chelate of 3-amino-5-oxo-5-phenylpent-3-enolhydrazide*benzene
CAS No.:951308-74-0
Molecular Formula:C₆H₆*C₃₅H₃₁B₂N₃O₂
Molecular Weight:625.386
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(phenylboron) chelate of 3-amino-5-oxo-5-phenylpent-3-enolhydrazide*benzene

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Technology Process of di(phenylboron) chelate of 3-amino-5-oxo-5-phenylpent-3-enolhydrazide*benzene

There total 1 articles about di(phenylboron) chelate of 3-amino-5-oxo-5-phenylpent-3-enolhydrazide*benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 3-amino-5-oxo-5-phenylpent-3-enolhydrazide

: 15323-04-3
diphenylborinic acid butyl ester

: 951308-74-0
di(phenylboron) chelate of 3-amino-5-oxo-5-phenylpent-3-enolhydrazide*benzene

Guidance literature:: In tetrahydrofuran; addn. of boron compd. to suspn. of hydrazide deriv. in THF, refluxing for 15 min, keeping at 20°C for 24 h; evapn., recrystn. (benzene/hexane (2:1)), filtration, washing with benzene/hexane (2:1), drying in vac., elem. anal.;
DOI:10.1007/s11172-006-0402-0