carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide

Base Information

Chemical Name:carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide
CAS No.:1344034-39-4
Molecular Formula:C₅₃H₆₃N₂O₇P
Molecular Weight:871.066
Hs Code.:

carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide

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Chemical Property of carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide

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Technology Process of carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide

There total 2 articles about carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1257084-30-2
carbonic acid 7,8-didehydro-1,2:5,6-dibenzocyclooctene-3-yl ester ((6'-hydroxy)hexyl)-1'-amide

: 1344034-39-4
carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 0.33 h / 20 °C / Inert atmosphere

2: 1H-tetrazole / 1,4-dioxane; acetonitrile / 0.5 h / 20 °C / Inert atmosphere

With 1H-tetrazole; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1055/s-0030-1260104

Reference yield:

: 56183-63-2
bis(diisopropylamino)chlorophosphine

: 1344034-39-4
carbonic acid 7,8-didehydro-1,2:5,6-dibenzocycloocten-3-yl ester, 6'-[3-O-(4,4'-dimethoxytrityl)-propanoxy-N,N'-diisopropylamino]phosphinooxy 1'-amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 0.33 h / 20 °C / Inert atmosphere

2: 1H-tetrazole / 1,4-dioxane; acetonitrile / 0.5 h / 20 °C / Inert atmosphere

With 1H-tetrazole; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1055/s-0030-1260104