CpTiCl₂NP(t)Bu₂(CH₂)3OCH₂Ph

Base Information

Chemical Name:CpTiCl₂NP(t)Bu₂(CH₂)3OCH₂Ph
CAS No.:1144517-05-4
Molecular Formula:C₂₃H₃₆Cl₂NOPTi
Molecular Weight:492.305
Hs Code.:

CpTiCl<sub>2</sub>NP(t)Bu<sub>2</sub>(CH<sub>2</sub>)3OCH<sub>2</sub>Ph

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Chemical Property of CpTiCl₂NP(t)Bu₂(CH₂)3OCH₂Ph

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Technology Process of CpTiCl₂NP(t)Bu₂(CH₂)3OCH₂Ph

There total 1 articles about CpTiCl₂NP(t)Bu₂(CH₂)3OCH₂Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 1144517-03-2
(Me₃SiN)tBuP(CH₂)3OCH₂Ph

: 1144517-05-4
CpTiCl₂NP(t)Bu₂(CH₂)3OCH₂Ph

Guidance literature:: In toluene; (N2); dropwise addn. of a soln. of ligand in toluene to a soln. of Ti complex in toluene, reflux overnight; evapn. in vac., addn. of hexanes, decantation, drying in vac.; elem. anal.;
DOI:10.1039/b817959j

Reference yield: 77.0%

: 1144517-05-4
CpTiCl₂NP(t)Bu₂(CH₂)3OCH₂Ph

: 917-54-4
methyllithium

: 1144517-09-8
CpTiMe₂NP(t)Bu₂(CH₂)3OCH₂Ph

Guidance literature:: In diethyl ether; benzene; byproducts: LiCl; (N2); dropwise addn. of a soln. of MeLi in ether to a soln. of Ti complex in benzene, stirring for 25 min; evapn. in vac., addn. of hexanes, filtration, evapn. in vac.; elem. anal.;
DOI:10.1039/b817959j