Co[di(1-phenyl-3-methyl-4-benzoylpyrazole-5-one semicarbazone] hydrate

Base Information

• Chemical Name: Co[di(1-phenyl-3-methyl-4-benzoylpyrazole-5-one semicarbazone] hydrate
• CAS No.: 866724-33-6
• Molecular Formula: C₃₆H₃₂CoN₁₀O₄*H₂O
• Molecular Weight: 745.723
• Mol file: 866724-33-6.mol

Synonyms:

Chemical Property of Co[di(1-phenyl-3-methyl-4-benzoylpyrazole-5-one semicarbazone] hydrate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Co[di(1-phenyl-3-methyl-4-benzoylpyrazole-5-one semicarbazone] hydrate

There total 1 articles about Co[di(1-phenyl-3-methyl-4-benzoylpyrazole-5-one semicarbazone] hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

cobalt(II) diacetate tetrahydrate (6147-53-1) + 4-benzoylsemicarbazone-1-phenyl-3-methyl-2-pyrazoline-5-one → Co[di(1-phenyl-3-methyl-4-benzoylpyrazole-5-one semicarbazone] hydrate (866724-33-6)

Guidance literature:

In ethanol; water; Co-compd. dissolved in H2O, warmed to 50°C, added to a warm ethanol solution of semicarbazone-compd. with stirring, heated under reflux for 0.5 h, cooled to room temp.; recrystd. from DMF/EtOH 1:4, filtered, washed with EtOH, dried in air, elem. anal.;

DOI:10.1081/SIM-200055235

upstream raw materials:

cobalt(II) diacetate tetrahydrate