ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl

Base Information

Chemical Name:ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl
CAS No.:936212-22-5
Molecular Formula:C₃₃H₂₈Fe₂
Molecular Weight:536.279
Hs Code.:

ferrocenylC(CH<sub>3</sub>)2ferrocenyl-C<sub>.</sub>tplbond.C-C<sub>.</sub>tplbond.C-phenyl

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Chemical Property of ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl

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Technology Process of ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl

There total 1 articles about ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 936212-23-6
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.CH

: 536-74-3
phenylacetylene

: 936212-22-5
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl

Guidance literature:: copper(l) chloride; In pyridine; (N2); Fe-compound, PhCCH and CuCl dissolved in C5H5N; soln. stirred for 3 h in air at 60°C; solvent removed under reduced pressure; mixt. washed with saturated NH4Cl soln.; extracted with CH2Cl2; organic phase dried over MgSO4; filtrated; filtrate concd.; residue chromatographed on neutral Al2O3; eluted with hexane/benzene (2:1); further steps;
DOI:10.1016/j.poly.2006.09.044

Reference yield: 28.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 936212-22-5
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl

: 12157-08-3
[(Co₂(CO)6)2(PhC_.tplbond.CC_.tplbond.CPh)]

: 936212-24-7,936212-18-9
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenylCo₂(CO)6

: 936212-18-9,936212-24-7
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenylCo₂(CO)6

: 936212-19-0
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl(Co₂(CO)6)2

Guidance literature:: In benzene; (N2); benzen soln. of Co2(CO)8 and Fe-compound stirred for 12 h at room temp.; solvent removed in vacuum; dissolved in benzene; residue chromatographedon silica gel column; eluted with hexane/benzene (5:1) afforded 4 bands ; elem. anal.;
DOI:10.1016/j.poly.2006.09.044

Reference yield: 24.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 936212-22-5
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl

: 936212-19-0
ferrocenylC(CH₃)2ferrocenyl-C_.tplbond.C-C_.tplbond.C-phenyl(Co₂(CO)6)2

Guidance literature:: In benzene; (N2); benzen soln. of Co2(CO)8 and Fe-compound stirred for 12 h at room temp.; solvent removed in vacuum; dissolved in benzene; residue chromatographedon silica gel column; eluted with hexane/benzene (5:1); recrystallized from hexane at -20°C; elem. anal.;
DOI:10.1016/j.poly.2006.09.044