Technology Process of C60H93NO22
There total 6 articles about C60H93NO22 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dmap; benzoyl chloride; triethylamine / tetrahydrofuran / 0 - 20 °C
2.1: acetic acid / water / 45 °C
3.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
4.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
5.1: 5%-palladium/activated carbon; hydrogen / tetrahydrofuran
6.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
6.2: 20 °C
With
dmap; 5%-palladium/activated carbon; hydrogen; benzoyl chloride; acetic acid; triethylamine; pivalic anhydride;
In
tetrahydrofuran; water;
DOI:10.1007/s11746-010-1675-x
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid / water / 45 °C
2.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
3.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
4.1: 5%-palladium/activated carbon; hydrogen / tetrahydrofuran
5.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
5.2: 20 °C
With
dmap; 5%-palladium/activated carbon; hydrogen; acetic acid; pivalic anhydride;
In
tetrahydrofuran; water;
DOI:10.1007/s11746-010-1675-x
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
2.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
3.1: 5%-palladium/activated carbon; hydrogen / tetrahydrofuran
4.1: dmap; pivalic anhydride / tetrahydrofuran / 20 °C
4.2: 20 °C
With
dmap; 5%-palladium/activated carbon; hydrogen; pivalic anhydride;
In
tetrahydrofuran;
DOI:10.1007/s11746-010-1675-x
