Technology Process of C26H20N2O6S
There total 5 articles about C26H20N2O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C
2: piperidine; sulfur / ethanol / 4 h / 50 °C
3: chloranil / 1,4-dioxane / 5 h / 90 °C
4: hydrogenchloride / butan-1-ol / 2 h / Reflux
5: water; sodium hydroxide / ethanol / 2 h / Reflux
With
piperidine; hydrogenchloride; palladium 10% on activated carbon; water; hydrogen; chloranil; sulfur; sodium hydroxide;
In
1,4-dioxane; ethanol; ethyl acetate; butan-1-ol;
2: Gewald reaction;
DOI:10.1016/j.tetlet.2010.12.081
- Guidance literature:
-
Multi-step reaction with 3 steps
1: chloranil / 1,4-dioxane / 5 h / 90 °C
2: hydrogenchloride / butan-1-ol / 2 h / Reflux
3: water; sodium hydroxide / ethanol / 2 h / Reflux
With
hydrogenchloride; water; chloranil; sodium hydroxide;
In
1,4-dioxane; ethanol; butan-1-ol;
DOI:10.1016/j.tetlet.2010.12.081
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / butan-1-ol / 2 h / Reflux
2: water; sodium hydroxide / ethanol / 2 h / Reflux
With
hydrogenchloride; water; sodium hydroxide;
In
ethanol; butan-1-ol;
DOI:10.1016/j.tetlet.2010.12.081
