(S)-Ph₂PNC₄H₄MeCH₂Ph

Base Information

Chemical Name:(S)-Ph₂PNC₄H₄MeCH₂Ph
CAS No.:1310488-74-4
Molecular Formula:C₂₄H₂₄NP
Molecular Weight:357.435
Hs Code.:

(S)-Ph<sub>2</sub>PNC<sub>4</sub>H<sub>4</sub>MeCH<sub>2</sub>Ph

Synonyms:

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Chemical Property of (S)-Ph₂PNC₄H₄MeCH₂Ph

Chemical Property:

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Technology Process of (S)-Ph₂PNC₄H₄MeCH₂Ph

There total 5 articles about (S)-Ph₂PNC₄H₄MeCH₂Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310488-88-0
C₁₂H₁₅N

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1310488-74-4
(S)-Ph₂PNC₄H₄MeCH₂Ph

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 9h;
DOI:10.1039/c1cc11823d

Reference yield:

: 1310488-75-5
C₁₇H₂₃NO₂

: 1310488-74-4
(S)-Ph₂PNC₄H₄MeCH₂Ph

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1.5 h / 20 °C

2: sodium hydroxide / diethyl ether; water

3: triethylamine / tetrahydrofuran / 9 h / 20 °C

With triethylamine; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1039/c1cc11823d

Reference yield:

: 1310488-87-9
C₁₉H₂₇NO₂

: 1310488-74-4
(S)-Ph₂PNC₄H₄MeCH₂Ph

Guidance literature:: Multi-step reaction with 4 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / benzene / 6 h / 60 °C

2: dichloromethane / 1.5 h / 20 °C

3: sodium hydroxide / diethyl ether; water

4: triethylamine / tetrahydrofuran / 9 h / 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; triethylamine; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene;
DOI:10.1039/c1cc11823d