C₂₃H₂₂FNO₄

Base Information

Chemical Name:C₂₃H₂₂FNO₄
CAS No.:1340596-41-9
Molecular Formula:C₂₃H₂₂FNO₄
Molecular Weight:395.43
Hs Code.:

C<sub>23</sub>H<sub>22</sub>FNO<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₃H₂₂FNO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₂FNO₄

Chemical Property:

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MSDS Files:

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Technology Process of C₂₃H₂₂FNO₄

There total 9 articles about C₂₃H₂₂FNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 459-56-3
4-fluorobenzylic alcohol

: 1340596-40-8
C₂₃H₂₂FNO₄

: 1340596-41-9
C₂₃H₂₂FNO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 25 °C

1.2: 12 h

2.1: acetic anhydride / 5 h / Reflux

2.2: 3 h / 60 °C

3.1: potassium phosphate; N,N`-dimethylethylenediamine / copper(l) iodide / 1,4-dioxane; tetrahydrofuran / 0.33 h / 160 °C / Microwave irradiation

4.1: ethanol; sodium tetrahydroborate / 1 h / 0 - 20 °C

5.1: Berger MultiGram_.(TM). SFC AD column / isopropyl alcohol; carbon dioxide / Resolution of racemate

With sodium tetrahydroborate; potassium phosphate; ethanol; acetic anhydride; sodium hydride; N,N`-dimethylethylenediamine; copper(l) iodide; In tetrahydrofuran; 1,4-dioxane; carbon dioxide; N,N-dimethyl-formamide; isopropyl alcohol; mineral oil;

Reference yield:

: 69267-75-0
2-bromo-1-cyclopropylethan-1-one

: 1340596-40-8
C₂₃H₂₂FNO₄

: 1340596-41-9
C₂₃H₂₂FNO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 0.17 h / 20 °C

1.2: 0.5 h

1.3: Cooling

2.1: potassium phosphate; N,N`-dimethylethylenediamine / copper(l) iodide / 1,4-dioxane; tetrahydrofuran / 0.33 h / 160 °C / Microwave irradiation

3.1: ethanol; sodium tetrahydroborate / 1 h / 0 - 20 °C

4.1: Berger MultiGram_.(TM). SFC AD column / isopropyl alcohol; carbon dioxide / Resolution of racemate

With sodium tetrahydroborate; potassium phosphate; ethanol; potassium tert-butylate; N,N`-dimethylethylenediamine; copper(l) iodide; In tetrahydrofuran; 1,4-dioxane; carbon dioxide; dimethyl sulfoxide; isopropyl alcohol;

Reference yield:

: 1340596-78-2
2-(4-bromophenoxy)-1-cyclopropylethanone

: 1340596-40-8
C₂₃H₂₂FNO₄

: 1340596-41-9
C₂₃H₂₂FNO₄

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate; N,N`-dimethylethylenediamine / copper(l) iodide / 1,4-dioxane; tetrahydrofuran / 0.33 h / 160 °C / Microwave irradiation

2: ethanol; sodium tetrahydroborate / 1 h / 0 - 20 °C

3: Berger MultiGram_.(TM). SFC AD column / isopropyl alcohol; carbon dioxide / Resolution of racemate

With sodium tetrahydroborate; potassium phosphate; ethanol; N,N`-dimethylethylenediamine; copper(l) iodide; In tetrahydrofuran; 1,4-dioxane; carbon dioxide; isopropyl alcohol;