C₅₃H₆₀N₆O₁₇

Base Information

Chemical Name:C₅₃H₆₀N₆O₁₇
CAS No.:135959-05-6
Molecular Formula:C₅₃H₆₀N₆O₁₇
Molecular Weight:1053.09
Hs Code.:

C<sub>53</sub>H<sub>60</sub>N<sub>6</sub>O<sub>17</sub>

Synonyms:

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Chemical Property of C₅₃H₆₀N₆O₁₇

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Technology Process of C₅₃H₆₀N₆O₁₇

There total 7 articles about C₅₃H₆₀N₆O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129193-26-6
C₆₁H₇₈N₆O₁₇Si

: 135959-05-6
C₅₃H₆₀N₆O₁₇

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)97368-4

Reference yield:

: 133510-57-3
5'-O-Levulinoyl-3'-O-(methylthiomethyl)thymidine

: 135959-05-6
C₅₃H₆₀N₆O₁₇

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / N-iodosuccinimide, 4A molecular sieves, TfOH / tetrahydrofuran; 1,2-dichloro-ethane / 0.08 h / 0 °C

2: 25percent aq. NH₃ / dioxane / 5 h / 50 °C

3: pyridine / 0.67 h / Ambient temperature

With pyridine; ammonium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In tetrahydrofuran; 1,4-dioxane; 1,2-dichloro-ethane;
DOI:10.1002/recl.19931120104

Reference yield:

: 17331-53-2
3'-O-benzoylthymidine

: 135959-05-6
C₅₃H₆₀N₆O₁₇

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / N-iodosuccinimide, 4A molecular sieves, TfOH / tetrahydrofuran; 1,2-dichloro-ethane / 0.05 h / 0 °C

2: 81 percent / N₂H₄*H₂O, pyridine, AcOH / 0.08 h / Ambient temperature

3: 80 percent / N-iodosuccinimide, 4A molecular sieves, TfOH / tetrahydrofuran; 1,2-dichloro-ethane / 0.08 h / 0 °C

4: 25percent aq. NH₃ / dioxane / 5 h / 50 °C

5: pyridine / 0.67 h / Ambient temperature

With pyridine; ammonium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; hydrazine hydrate; acetic acid; In tetrahydrofuran; 1,4-dioxane; 1,2-dichloro-ethane;
DOI:10.1002/recl.19931120104