2--4-phenylthiazole

Base Information

• Chemical Name: 2--4-phenylthiazole
• CAS No.: 58350-95-1
• Molecular Formula: C₁₄H₁₂N₂O₂S
• Molecular Weight: 272.327

Synonyms:

Chemical Property of 2--4-phenylthiazole

Chemical Property:

Purity/Quality:

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Technology Process of 2--4-phenylthiazole

There total 2 articles about 2--4-phenylthiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-oxo-2-phenylethylthiocyanate (5399-30-4) + ethyl 2-cyanoacetate (105-56-6) → 2--4-phenylthiazole (58350-95-1)

Guidance literature:

With piperidine; for 2h; Heating;

Reference yield:

5-phenyl-2,3-dihydro-thiazolo[2,3-b]thiazolylium; bromide (6094-68-4) + ethyl 2-cyanoacetate (105-56-6) → 2--4-phenylthiazole (58350-95-1)

Guidance literature:

Multistep reaction; (i) NaH, benzene, (ii) /BRN= 4050648/, DMF;

DOI:10.1248/cpb.23.3254

Reference yield: 55.0%

2--4-phenylthiazole (58350-95-1) → 5-Amino-2-phenyl-4-(4-phenyl-thiazol-2-yl)-2H-pyrazol-3-ol

Guidance literature:

With triethylamine; In 1,4-dioxane; for 2h; Heating;

upstream raw materials:

5-phenyl-2,3-dihydro-thiazolo[2,3-b]thiazolylium; bromide

ethyl 2-cyanoacetate

2-oxo-2-phenylethylthiocyanate

Downstream raw materials:

2-cyano-2-(4-phenyl-thiazol-2-yl)-propionic acid ethyl ester

2-(4-phenyl-thiazol-2-yl)-propionitrile

ethyl-2 phenyl-4 thiazole

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