epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine

Base Information

Chemical Name:epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine
CAS No.:948915-99-9
Molecular Formula:C₁₈H₂₄N₁₂O₉
Molecular Weight:552.464
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine

Chemical Property:

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Technology Process of epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine

There total 2 articles about epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₃F₃N₁₂O₁₁S

: 948915-99-9
epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine

Guidance literature:: With 15-crown-5; sodium nitrite; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2007.06.002

Reference yield:

: 182554-04-7
1,3,2′,6′-tetraazido-6,3′,4′-tri-O-acetylneamine

: 948915-99-9
epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.05 g / pyridine; CH₂Cl₂ / 1.5 h / 20 °C

2: 0.57 g / NaNO₂; 15-crown-5 / dimethylformamide / 24 h / 20 °C

With 15-crown-5; sodium nitrite; In pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.06.002

Reference yield: 23.0%

: 948915-99-9
epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine

: 358-23-6
trifluoromethylsulfonic anhydride

: 109-76-2,54018-94-9
Trimethylenediamine

: 948916-24-3
5-(3-aminopropyl)-amino-1,3,2',6'-tetraazido neamine

Guidance literature:: epi-5-hydroxyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-acetyl neamine; trifluoromethylsulfonic anhydride; In pyridine; dichloromethane; at 20 ℃; for 1.5h;

Trimethylenediamine; In tetrahydrofuran; at 20 ℃; for 24h; Further stages.;
DOI:10.1016/j.tet.2007.06.002