C₃₂H₂₉BrN₂O₇

Base Information

Chemical Name:C₃₂H₂₉BrN₂O₇
CAS No.:1014005-24-3
Molecular Formula:C₃₂H₂₉BrN₂O₇
Molecular Weight:633.495
Hs Code.:

C<sub>32</sub>H<sub>29</sub>BrN<sub>2</sub>O<sub>7</sub>

Synonyms:

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Chemical Property of C₃₂H₂₉BrN₂O₇

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Technology Process of C₃₂H₂₉BrN₂O₇

There total 6 articles about C₃₂H₂₉BrN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61-54-1
tryptamine

: 958848-26-5
C₂₂H₁₉BrO₈

: 1014005-24-3
C₃₂H₂₉BrN₂O₇

Guidance literature:: tryptamine; C₂₂H₁₉BrO₈; In water; acetonitrile; at 20 ℃; for 8h; Inert atmosphere;

In water; acetonitrile; at 120 ℃; for 0.25h; Inert atmosphere;

With Amberlite IRC₇₆ resin; In water; acetonitrile; at 120 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/co300002x

Reference yield:

: 1361317-32-9
6-(hex-1-ynyl)-2,4-dihydroxy-3-methylbenzaldehyde

: 1014005-24-3
C₃₂H₂₉BrN₂O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: Au(OAc)3 / 1,2-dichloro-ethane / 0.17 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 1.5 h / 20 °C / Inert atmosphere

3.1: N-Bromosuccinimide / acetonitrile / 1 h / 20 °C / Inert atmosphere

4.1: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere

5.1: water; acetonitrile / 8 h / 20 °C / Inert atmosphere

5.2: 0.25 h / 120 °C / Inert atmosphere

5.3: Amberlite IRC₇₆ resin / 0.25 h / 120 °C / Inert atmosphere

With N-Bromosuccinimide; Au(OAc)3; tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/co300002x

Reference yield:

: 1014007-85-2
C₁₄H₁₆O₄

: 1014005-24-3
C₃₂H₂₉BrN₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / acetonitrile / 1 h / 20 °C / Inert atmosphere

2.1: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere

3.1: water; acetonitrile / 8 h / 20 °C / Inert atmosphere

3.2: 0.25 h / 120 °C / Inert atmosphere

3.3: Amberlite IRC₇₆ resin / 0.25 h / 120 °C / Inert atmosphere

With N-Bromosuccinimide; In dichloromethane; water; acetonitrile;
DOI:10.1021/co300002x