2,3,6-Tris-(trifluormethyl)-benzoylfluorid

Base Information

• Chemical Name: 2,3,6-Tris-(trifluormethyl)-benzoylfluorid
• CAS No.: 41819-01-6
• Molecular Formula: C₁₀H₂F₁₀O
• Molecular Weight: 328.109
• Mol file: 41819-01-6.mol

Synonyms:

Chemical Property of 2,3,6-Tris-(trifluormethyl)-benzoylfluorid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,6-Tris-(trifluormethyl)-benzoylfluorid

There total 5 articles about 2,3,6-Tris-(trifluormethyl)-benzoylfluorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Trifluormethyl-trimellithsaeure (41819-00-5) → 2,3,6-Tris-(trifluormethyl)-benzoylfluorid (41819-01-6)

Guidance literature:

With sulfur tetrafluoride; at 100 - 220 ℃;

Reference yield:

3,5-Dimethyl-4-trifluormethyl-benzoesaeure (3360-57-4) → 2,3,6-Tris-(trifluormethyl)-benzoylfluorid (41819-01-6)

Guidance literature:

Multi-step reaction with 5 steps

1: Cu / quinoline / 250 °C

2: aq. H₂SO₄

3: aq. HNO₃

4: aq. KOH, KMnO₄

5: SF₄ / 100 - 220 °C

With potassium hydroxide; potassium permanganate; sulfuric acid; sulfur tetrafluoride; nitric acid; copper; In quinoline;

Reference yield:

1,3-dimethyl-2-(trifluoromethyl)benzene (41818-96-6) → 2,3,6-Tris-(trifluormethyl)-benzoylfluorid (41819-01-6)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. H₂SO₄

2: aq. HNO₃

3: aq. KOH, KMnO₄

4: SF₄ / 100 - 220 °C

With potassium hydroxide; potassium permanganate; sulfuric acid; sulfur tetrafluoride; nitric acid;

upstream raw materials:

3-Trifluormethyl-trimellithsaeure

1,3-dimethyl-2-(trifluoromethyl)benzene

3-Chlormethyl-2.6-dimethylbenzotrifluorid

3,5-Dimethyl-4-trifluormethyl-benzoesaeure

Downstream raw materials:

1,2,4-tris-(trifluoromethyl)-benzene

2,3,6-tris(trifluoromethyl)benzonitrile

2,3,6-Tris-(trifluormethyl)-benzoesaeure

2,3,6-Tris-(trifluormethyl)-benzamid