Technology Process of aflatoxin B2
There total 9 articles about aflatoxin B2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
1,4-dioxane;
Ambient temperature;
DOI:10.1039/c39900000039
- Guidance literature:
-
Multi-step reaction with 7 steps
1: benzyltrimethylammonium dichloroiodate / methanol; CH2Cl2
2: 1.) NaH, 2.) n-BuLi / 1.) 0 deg C, 2.) -100 deg C, 15 min
3: K2CO3
5: H2 / 30percent Pd/C / ethyl acetate / 9 h / 10343 Torr
6: trifluoroacetic acid / CH2Cl2 / Ambient temperature
7: 100 percent / dichloro dicyano benzoquinone / dioxane / Ambient temperature
With
n-butyllithium; hydrogen; sodium hydride; potassium carbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
palladium on activated charcoal;
In
1,4-dioxane; methanol; dichloromethane; ethyl acetate;
DOI:10.1039/c39900000039
- Guidance literature:
-
Multi-step reaction with 5 steps
1: K2CO3
3: H2 / 30percent Pd/C / ethyl acetate / 9 h / 10343 Torr
4: trifluoroacetic acid / CH2Cl2 / Ambient temperature
5: 100 percent / dichloro dicyano benzoquinone / dioxane / Ambient temperature
With
hydrogen; potassium carbonate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
palladium on activated charcoal;
In
1,4-dioxane; dichloromethane; ethyl acetate;
DOI:10.1039/c39900000039
