{(1,1,1-tris(diphenylphosphinomethyl)ethane)Co(O₂SO)}

Base Information

• Chemical Name: {(1,1,1-tris(diphenylphosphinomethyl)ethane)Co(O₂SO)}
• CAS No.: 109111-98-0
• Molecular Formula: C₄₁H₃₉CoO₃P₃S
• Molecular Weight: 763.739

Synonyms:

Chemical Property of {(1,1,1-tris(diphenylphosphinomethyl)ethane)Co(O₂SO)}

Chemical Property:

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Technology Process of {(1,1,1-tris(diphenylphosphinomethyl)ethane)Co(O₂SO)}

There total 1 articles about {(1,1,1-tris(diphenylphosphinomethyl)ethane)Co(O₂SO)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

{(1,1,1-tris(diphenylphosphinomethyl)ethane)Co(μ-Cl)2Co(1,1,1-tris(diphenylphophinomethyl)ethane)}(2+) → {(1,1,1-tris(diphenylphosphinomethyl)ethane)Co(O2SO)} (109111-98-0)

Guidance literature:

With sodium amalgame; SO₂; In tetrahydrofuran; byproducts: NaCl; THF soln., Na/Hg under N2; SO2 was bubbled through a soln. for two min;; butanol was added; evapd., ppt. was filtered off, washed with butanol and petroleum ether, dried in a stream of N2; recrystd. from CH2Cl2-butanol;;

DOI:10.1016/0022-328X(87)87136-X

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