C₂₂H₂₃N₃O₂

Base Information

Chemical Name:C₂₂H₂₃N₃O₂
CAS No.:1403755-17-8
Molecular Formula:C₂₂H₂₃N₃O₂
Molecular Weight:361.444
Hs Code.:

C<sub>22</sub>H<sub>23</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₃N₃O₂

Chemical Property:

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Technology Process of C₂₂H₂₃N₃O₂

There total 5 articles about C₂₂H₂₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41423-61-4
6-acetyl-3,4-dihydro-7-methoxy-2,2-dimethyl-2H-benzopyran

: 1403755-17-8
C₂₂H₂₃N₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / 1,4-dioxane / 20 °C

2: sodium methylate / methanol / Reflux

With boron trifluoride diethyl etherate; sodium methylate; In 1,4-dioxane; methanol; 1: Claisen-Schmidt condensation;
DOI:10.2298/JSC110923008M

Reference yield:

: 31005-72-8
2,2-dimethylchroman-7-ol

: 1403755-17-8
C₂₂H₂₃N₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: zinc(II) chloride / 0.25 h / 140 - 150 °C

2: potassium carbonate / acetone / 2 h / 20 °C

3: boron trifluoride diethyl etherate / 1,4-dioxane / 20 °C

4: sodium methylate / methanol / Reflux

With boron trifluoride diethyl etherate; sodium methylate; potassium carbonate; zinc(II) chloride; In 1,4-dioxane; methanol; acetone; 3: Claisen-Schmidt condensation;
DOI:10.2298/JSC110923008M

Reference yield:

: 108-46-3
recorcinol

: 1403755-17-8
C₂₂H₂₃N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: polyphosphoric acid / dichloromethane / 5 h / 20 °C / Reflux

2: zinc(II) chloride / 0.25 h / 140 - 150 °C

3: potassium carbonate / acetone / 2 h / 20 °C

4: boron trifluoride diethyl etherate / 1,4-dioxane / 20 °C

5: sodium methylate / methanol / Reflux

With boron trifluoride diethyl etherate; sodium methylate; potassium carbonate; zinc(II) chloride; In 1,4-dioxane; methanol; dichloromethane; acetone; 4: Claisen-Schmidt condensation;
DOI:10.2298/JSC110923008M