α-dihydro grayanotoxin-II

Base Information

Chemical Name:α-dihydro grayanotoxin-II
CAS No.:104528-31-6
Molecular Formula:C₂₀H₃₄O₅
Molecular Weight:354.487
Hs Code.:

Synonyms:

Suppliers and Price of α-dihydro grayanotoxin-II

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-dihydro grayanotoxin-II

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of α-dihydro grayanotoxin-II

There total 5 articles about α-dihydro grayanotoxin-II which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: grayanotoxin-II

: 38776-76-0,38776-77-1,78185-87-2,104528-31-6,149819-17-0,149819-21-6
α-dihydro grayanotoxin-II

Guidance literature:: With hydrogen; palladium; In ethanol; acetic acid;
DOI:10.1271/bbb1961.45.2483

Reference yield:

: 66656-59-5,66701-64-2
α-Dihydrograyanotoxin-II-tetraacetat

: 38776-76-0,38776-77-1,78185-87-2,104528-31-6,149819-17-0,149819-21-6
α-dihydro grayanotoxin-II

Guidance literature:: Multi-step reaction with 4 steps

1: 5percent aq. K₂CO₃ / methanol / 48 h / Ambient temperature

2: methanesulphjonyl chloride / pyridine

3: MCPBA / CH₂Cl₂ / 10 h / Ambient temperature

4: lithium aluminium hydride

With lithium aluminium tetrahydride; potassium carbonate; methanesulfonyl chloride; 3-chloro-benzenecarboperoxoic acid; In pyridine; methanol; dichloromethane;
DOI:10.1271/bbb1961.45.2483

Reference yield:

: C₂₆H₃₈O₇

: 38776-76-0,38776-77-1,78185-87-2,104528-31-6,149819-17-0,149819-21-6
α-dihydro grayanotoxin-II

Guidance literature:: Multi-step reaction with 2 steps

1: MCPBA / CH₂Cl₂ / 10 h / Ambient temperature

2: lithium aluminium hydride

With lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1271/bbb1961.45.2483