phenyl (di-tert-butyl)phosphinate

Base Information

• Chemical Name: phenyl (di-tert-butyl)phosphinate
• CAS No.: 27286-05-1
• Molecular Formula: C₁₄H₂₃O₂P
• Molecular Weight: 254.309
• Mol file: 27286-05-1.mol

Synonyms:

Chemical Property of phenyl (di-tert-butyl)phosphinate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl (di-tert-butyl)phosphinate

There total 4 articles about phenyl (di-tert-butyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-tris(di-tert-butylphosphinooxy)benzene (1203843-07-5) → phenyl (di-tert-butyl)phosphinate (27286-05-1)

Guidance literature:

1,3,5-tris(di-tert-butylphosphinooxy)benzene;

With aluminum oxide; In toluene; for 2h; Inert atmosphere;

DOI:10.1039/c0dt01369b

Reference yield:

di(tert-butyl)chlorophosphine (13716-10-4) → phenyl (di-tert-butyl)phosphinate (27286-05-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide

2: (i) Cl₂, CCl₄, (ii) MeOH

In N,N-dimethyl-formamide;

DOI:10.1039/j39700001263

Reference yield:

sodium phenoxide (139-02-6) → phenyl (di-tert-butyl)phosphinate (27286-05-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide

2: (i) Cl₂, CCl₄, (ii) MeOH

In N,N-dimethyl-formamide;

DOI:10.1039/j39700001263

upstream raw materials:

phenyl di(tert-butyl)phosphinite

di(tert-butyl)chlorophosphine

sodium phenoxide

1,3,5-tris(di-tert-butylphosphinooxy)benzene