3-amino-N-(2,4-dichlorophenyl)-3-thioxopropanamide

Base Information

Chemical Name:3-amino-N-(2,4-dichlorophenyl)-3-thioxopropanamide
CAS No.:102817-88-9
Molecular Formula:C9H8Cl2N2OS
Molecular Weight:263.147
Hs Code.:
DSSTox Substance ID:DTXSID201226120
Mol file:102817-88-9.mol

Synonyms:3-amino-N-(2,4-dichlorophenyl)-3-thioxopropanamide;102817-88-9;DTXSID201226120

Suppliers and Price of 3-amino-N-(2,4-dichlorophenyl)-3-thioxopropanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-amino-N-(2,4-dichlorophenyl)-3-thioxopropanamide

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:261.9734394
Heavy Atom Count:15
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)Cl)NC(=O)CC(=S)N

Technology Process of 3-amino-N-(2,4-dichlorophenyl)-3-thioxopropanamide

There total 1 articles about 3-amino-N-(2,4-dichlorophenyl)-3-thioxopropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 17722-32-6
N-(2,4-dichlorophenyl)-2-cyanoacetamide

: 102817-88-9
N-(2,4-Dichloro-phenyl)-2-thiocarbamoyl-acetamide

Guidance literature:: With hydrogen sulfide; triethylamine; In pyridine;
DOI:10.1055/s-1985-31365

Reference yield: 83.0%

: 102817-88-9
N-(2,4-Dichloro-phenyl)-2-thiocarbamoyl-acetamide

: 123-54-6,81235-32-7
acetylacetone

: 102817-99-2
4,6-Dimethyl-2-thioxo-1,2-dihydro-pyridine-3-carboxylic acid (2,4-dichloro-phenyl)-amide

Guidance literature:: With triethylamine; In ethanol; for 24h; Heating;
DOI:10.1055/s-1985-31365

Reference yield:

: 102817-88-9
N-(2,4-Dichloro-phenyl)-2-thiocarbamoyl-acetamide

: 102818-19-9
2-(2,4-Dichloro-phenyl)-4,6-dimethyl-1-oxo-1,2-dihydro-1λ⁴-isothiazolo[5,4-b]pyridin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / (C₂H₅)3N / ethanol / 24 h / Heating

2: 90 percent / NaOH, potassium hexacyanoferrate(III) / Ambient temperature

3: 84 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 1.) -10 deg C, 2 h, 2.) room temp., overnight

With sodium hydroxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hexacyanoferrate(III); In ethanol; dichloromethane;
DOI:10.1055/s-1985-31365