2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl

Base Information

• Chemical Name: 2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl
• CAS No.: 106301-85-3
• Molecular Formula: C₃₃H₁₆Br₄Cl
• Molecular Weight: 767.559
• Mol file: 106301-85-3.mol

Synonyms:

Chemical Property of 2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl

There total 3 articles about 2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-Brom-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-propen-(1) (96975-31-4) → 2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl (106301-85-3)

Guidance literature:

With sodium hydroxide; potassium hexacyanoferrate(III); In N,N-dimethyl-formamide;

DOI:10.1007/BF00909246

Reference yield:

2,7-dibromo-9H-fluorene (16433-88-8) → 2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl (106301-85-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) KOMe, DMF, (ii) O₂

2: K₃, aq. NaOH / dimethylformamide

With sodium hydroxide; potassium hexacyanoferrate(III); In N,N-dimethyl-formamide;

DOI:10.1007/BF00909246

Reference yield:

2,7-dibromo-9-(4-chloro-benzylidene)-fluorene (65550-88-1) → 2-(4-Chlor-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-allyl (106301-85-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) KOMe, DMF, (ii) O₂

2: K₃, aq. NaOH / dimethylformamide

With sodium hydroxide; potassium hexacyanoferrate(III); In N,N-dimethyl-formamide;

DOI:10.1007/BF00909246

upstream raw materials:

2-(4-Brom-phenyl)-1,1,3,3-bis-(4,4'-dibrom-biphenylen)-propen-⁽¹⁾

2,7-dibromo-9H-fluorene

2,7-dibromo-9-(4-chloro-benzylidene)-fluorene