C₄₄H₅₅NO₂₈

Base Information

• Chemical Name: C₄₄H₅₅NO₂₈
• CAS No.: 1402245-98-0
• Molecular Formula: C₄₄H₅₅NO₂₈
• Molecular Weight: 1045.91
• Mol file: 1402245-98-0.mol

Synonyms:

Chemical Property of C₄₄H₅₅NO₂₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₅₅NO₂₈

There total 4 articles about C₄₄H₅₅NO₂₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4,6-tetra-O-acetyl-β-D-mannopyranosyl fluoride (439-03-2,439-04-3,439-05-4,2823-44-1,2823-46-3,3934-29-0,4163-44-4,4163-45-5,20409-31-8,23235-96-3,51897-75-7,51897-76-8,51897-77-9,62561-28-8,126641-47-2,57573-38-3) → C44H55NO28 (1402245-98-0)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonia / methanol / 4 h / 4 °C

2: mutant malA D₃₂₀G from Sulfolobus solfataricus / 96 h / 20 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

3: pyridine / 48 h / 20 °C

With pyridine; mutant malA D₃₂₀G from Sulfolobus solfataricus; ammonia; In methanol;

DOI:10.1002/anie.201201081

Reference yield:

β-D-mannopyranosyl fluoride (210281-95-1) → C44H55NO28 (1402245-98-0)

Guidance literature:

Multi-step reaction with 2 steps

1: mutant malA D₃₂₀G from Sulfolobus solfataricus / 96 h / 20 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

2: pyridine / 48 h / 20 °C

With pyridine; mutant malA D₃₂₀G from Sulfolobus solfataricus;

DOI:10.1002/anie.201201081

Reference yield:

C24H35NO18 (1402245-87-7) + acetic anhydride (108-24-7) → C44H55NO28 (1402245-98-0)

Guidance literature:

With pyridine; at 20 ℃; for 48h;

DOI:10.1002/anie.201201081

upstream raw materials:

C₂₄H₃₅NO₁₈

acetic anhydride

2,3,4,6-tetra-O-acetyl-β-D-mannopyranosyl fluoride

p-nitrophenyl 3-O-α-D-mannopyranosyl-α-D-mannopyranoside

Refernces