C₃₀H₃₆N₂O₆Te

Base Information

Chemical Name:C₃₀H₃₆N₂O₆Te
CAS No.:1430324-63-2
Molecular Formula:C₃₀H₃₆N₂O₆Te
Molecular Weight:648.226
Hs Code.:

C<sub>30</sub>H<sub>36</sub>N<sub>2</sub>O<sub>6</sub>Te

Synonyms:

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Chemical Property of C₃₀H₃₆N₂O₆Te

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Technology Process of C₃₀H₃₆N₂O₆Te

There total 5 articles about C₃₀H₃₆N₂O₆Te which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 32294-60-3
diphenyl ditelluride

: 1430324-62-1
C₂₄H₃₂N₂O₇

: 1430324-63-2
C₃₀H₃₆N₂O₆Te

Guidance literature:: diphenyl ditelluride; With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 0.666667h;

C₂₄H₃₂N₂O₇; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; methanol; for 0.333333h;
DOI:10.1021/ja402933s

Reference yield:

: 380358-27-0
3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole

: 1430324-63-2
C₃₀H₃₆N₂O₆Te

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

1.2: 0.5 h / 0 °C

2.1: n-butyllithium / 1,2-dimethoxyethane / 3 h / -78 - -40 °C / Schlenk technique; Inert atmosphere

2.2: 1.5 h / -78 - 20 °C / Schlenk technique; Inert atmosphere

2.3: 1 h / 20 °C / Schlenk technique; Inert atmosphere

3.1: (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate / acetonitrile / 0.08 h / -20 °C

3.2: 6 h / -20 °C

4.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; water / tetrahydrofuran; tert-butyl alcohol / 1.33 h / 0 °C

5.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.67 h

5.2: 0.33 h

With sodium chlorite; sodium tetrahydroborate; n-butyllithium; sodium dihydrogen phosphate monohydrate; (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate; water; sodium hydride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; N,N-dimethyl-formamide; acetonitrile; mineral oil; tert-butyl alcohol;
DOI:10.1021/ja402933s

Reference yield:

: tert-butyl (2-(5-methoxy-1-methyl-1H-indol-3-yl)ethyl)carbamate

: 1430324-63-2
C₃₀H₃₆N₂O₆Te

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / 1,2-dimethoxyethane / 3 h / -78 - -40 °C / Schlenk technique; Inert atmosphere

1.2: 1.5 h / -78 - 20 °C / Schlenk technique; Inert atmosphere

1.3: 1 h / 20 °C / Schlenk technique; Inert atmosphere

2.1: (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate / acetonitrile / 0.08 h / -20 °C

2.2: 6 h / -20 °C

3.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; water / tetrahydrofuran; tert-butyl alcohol / 1.33 h / 0 °C

4.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.67 h

4.2: 0.33 h

With sodium chlorite; sodium tetrahydroborate; n-butyllithium; sodium dihydrogen phosphate monohydrate; (5S)-5-benzyl-2,2,3-trimethyl-4-oxoimidazolidin-1-ium Tetrafluoroborate; water; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja402933s