Technology Process of C29H41NO5Si
There total 6 articles about C29H41NO5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; palladium dichloride;
In
tetrahydrofuran;
at 20 ℃;
for 36h;
DOI:10.1002/ejoc.201200384
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: lithium borohydride / tetrahydrofuran; methanol / 4.5 h / 0 - 20 °C / Inert atmosphere
1.2: 0 °C
2.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere
3.1: sodium azide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere
4.1: toluene / 24 h / 140 °C / Sealed tube; Inert atmosphere
5.1: sodium tetrahydroborate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere
6.1: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C / Inert atmosphere
7.1: water; palladium dichloride / tetrahydrofuran / 36 h / 20 °C
With
sodium tetrahydroborate; lithium borohydride; sodium azide; water; triethylamine; palladium dichloride;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.201200384
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere
2: sodium azide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere
3: toluene / 24 h / 140 °C / Sealed tube; Inert atmosphere
4: sodium tetrahydroborate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere
5: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C / Inert atmosphere
6: water; palladium dichloride / tetrahydrofuran / 36 h / 20 °C
With
sodium tetrahydroborate; sodium azide; water; triethylamine; palladium dichloride;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.201200384