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C28H43NO4Si

Base Information
  • Chemical Name:C28H43NO4Si
  • CAS No.:1438399-49-5
  • Molecular Formula:C28H43NO4Si
  • Molecular Weight:485.739
  • Hs Code.:
C<sub>28</sub>H<sub>43</sub>NO<sub>4</sub>Si

Synonyms:

Suppliers and Price of C28H43NO4Si
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Chemical Property of C28H43NO4Si
Chemical Property:
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Technology Process of C28H43NO4Si

There total 3 articles about C28H43NO4Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With camphor-10-sulfonic acid; In methanol; dichloromethane; at 0 ℃; for 6h;
DOI:10.1002/chem.201201332
Guidance literature:
Multi-step reaction with 6 steps
1.1: copper(l) iodide; methyllithium / tetrahydrofuran; diethyl ether / 8 h / 0 °C / Inert atmosphere
1.2: 0.5 h / 0 °C / Inert atmosphere
2.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / 0 - 25 °C / Inert atmosphere
3.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C
4.1: dichloromethane / 12 h / 25 °C / Inert atmosphere
5.1: copper(l) iodide; methyllithium / tetrahydrofuran; diethyl ether / 8 h / 0 °C / Inert atmosphere
5.2: 0 °C / Inert atmosphere
6.1: camphor-10-sulfonic acid / methanol; dichloromethane / 6 h / 0 °C
With copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid; methyllithium; lithium triethylborohydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1002/chem.201201332
Guidance literature:
Multi-step reaction with 5 steps
1.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / 0 - 25 °C / Inert atmosphere
2.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C
3.1: dichloromethane / 12 h / 25 °C / Inert atmosphere
4.1: copper(l) iodide; methyllithium / tetrahydrofuran; diethyl ether / 8 h / 0 °C / Inert atmosphere
4.2: 0 °C / Inert atmosphere
5.1: camphor-10-sulfonic acid / methanol; dichloromethane / 6 h / 0 °C
With copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid; methyllithium; lithium triethylborohydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1002/chem.201201332
upstream raw materials:

C30H43NO4SSi

C37H61NO4SSi2

C34H57NO4Si2

Downstream raw materials:

C31H47NO4Si

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