10-methylacridine-9(10H)-thione

Base Information

• Chemical Name: 10-methylacridine-9(10H)-thione
• CAS No.: 17435-19-7
• Molecular Formula: C14H11 N S
• Molecular Weight: 225.314
• Mol file: 17435-19-7.mol

Synonyms:9-Acridanthione,10-methyl- (6CI,7CI,8CI); 10-Methyl-9(10H)-acridinethione;N-Methylacridine-9-thione; N-Methylthioacridone; NSC 302575

Chemical Property of 10-methylacridine-9(10H)-thione

Chemical Property:

• Vapor Pressure: 1.35E-05mmHg at 25°C
• Boiling Point: 367.6°Cat760mmHg
• Flash Point: 176.1°C
• Density: 1.28g/cm³

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 10-methylacridine-9(10H)-thione

There total 7 articles about 10-methylacridine-9(10H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

10-methyl-9, 10-dihydro-9-acridinone (719-54-0) → N-methylthioacridone (17435-19-7)

Guidance literature:

With diphosphorus pentasulfide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 115 ℃; for 3.5h;

DOI:10.1055/s-1982-29851

Reference yield: 82.0%

10,10'-dimethyl-9,9'-biacridylidene (23663-77-6) → N-methylthioacridone (17435-19-7)

Guidance literature:

With sulfur; In toluene; for 6h; Heating; Irradiation; under CO₂;

DOI:10.1016/S0040-4020(01)87036-8

Reference yield: 61.0%

10-Methyl-9-trifluormethansulfonyloxyacridinium-trifluormethansulfonat (95256-32-9) → N-methylthioacridone (17435-19-7)

Guidance literature:

With sodium hydrogensulfide; In acetonitrile;

upstream raw materials:

10,10'-dimethyl-9,9'-biacridylidene

10-methyl-9, 10-dihydro-9-acridinone

C₁₈H₁₆N₂S

10-Methyl-9-trifluormethansulfonyloxyacridinium-trifluormethansulfonat

Downstream raw materials:

10-methyl-9, 10-dihydro-9-acridinone