[10,10-2H2]-1-bromoundecane

Base Information

Chemical Name:[10,10-2H2]-1-bromoundecane
CAS No.:386223-64-9
Molecular Formula:C₁₁H₂₃Br
Molecular Weight:237.192
Hs Code.:

Synonyms:

Suppliers and Price of [10,10-2H2]-1-bromoundecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [10,10-2H2]-1-bromoundecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [10,10-2H2]-1-bromoundecane

There total 8 articles about [10,10-2H2]-1-bromoundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 386223-62-7
[10,10-2H₂]-1-undecanol

: 386223-64-9
[10,10-2H2]-1-bromoundecane

Guidance literature:: With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 50 ℃; for 0.25h;
DOI:10.1021/jo010560w

Reference yield:

: 50816-19-8
8-bromooctanol

: 386223-64-9
[10,10-2H2]-1-bromoundecane

Guidance literature:: Multi-step reaction with 8 steps

1: 97 percent / LiBr; p-toluenesulfonic acid / 16 h / 20 °C

2: 60 percent / Na / ethanol / 26 h / Heating

3: 60 percent / Na / ethanol; ethane-1,2-diol / 0.5 h / 85 - 90 °C

4: 95 percent / NaBD₄ / methanol / 1 h / 20 °C

5: 73 percent / trimethylamine hydrochloride; triethylamine / CH₂Cl₂ / 1.5 h / 0 °C

6: LiAlD₄ / diethyl ether / 3 h / 20 °C

7: 108 mg / HCl / methanol / 16 h / 20 °C

8: 70 percent / N-bromosuccinimide / dimethylformamide / 0.25 h / 50 °C

With hydrogenchloride; N-Bromosuccinimide; lithium aluminium deuteride; sodium borodeuteride; sodium; trimethylamine hydrochloride; toluene-4-sulfonic acid; triethylamine; lithium bromide; In methanol; diethyl ether; ethanol; dichloromethane; ethylene glycol; N,N-dimethyl-formamide;
DOI:10.1021/jo010560w

Reference yield:

: 194926-03-9
1-bromo-8-methoxymethoxy-octane

: 386223-64-9
[10,10-2H2]-1-bromoundecane

Guidance literature:: Multi-step reaction with 7 steps

1: 60 percent / Na / ethanol / 26 h / Heating

2: 60 percent / Na / ethanol; ethane-1,2-diol / 0.5 h / 85 - 90 °C

3: 95 percent / NaBD₄ / methanol / 1 h / 20 °C

4: 73 percent / trimethylamine hydrochloride; triethylamine / CH₂Cl₂ / 1.5 h / 0 °C

5: LiAlD₄ / diethyl ether / 3 h / 20 °C

6: 108 mg / HCl / methanol / 16 h / 20 °C

7: 70 percent / N-bromosuccinimide / dimethylformamide / 0.25 h / 50 °C

With hydrogenchloride; N-Bromosuccinimide; lithium aluminium deuteride; sodium borodeuteride; sodium; trimethylamine hydrochloride; triethylamine; In methanol; diethyl ether; ethanol; dichloromethane; ethylene glycol; N,N-dimethyl-formamide;
DOI:10.1021/jo010560w