Technology Process of C24H26N4O4
There total 5 articles about C24H26N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride;
In
methanol; dichloromethane;
at 120 ℃;
for 0.333333h;
Microwave irradiation;
DOI:10.1021/co200062n
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bromine; sodium acetate / acetic acid / 20 °C
2: hydrogen bromide; bromine; sodium nitrite / water; acetic acid / 0.83 h / 0 - 5 °C
3: methanol / 1 h / 100 °C
4: di-tert-butyl-diazodicarboxylate / dichloromethane / 0.5 h / 20 °C
5: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride / methanol; dichloromethane / 0.33 h / 120 °C / Microwave irradiation
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; di-tert-butyl-diazodicarboxylate; hydrogen bromide; bromine; sodium acetate; cesium fluoride; sodium nitrite;
In
methanol; dichloromethane; water; acetic acid;
2: Sandmeyer reaction / 4: Mitsunobu reaction / 5: Suzuki coupling;
DOI:10.1021/co200062n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: di-tert-butyl-diazodicarboxylate / dichloromethane / 0.5 h / 20 °C
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride / methanol; dichloromethane / 0.33 h / 120 °C / Microwave irradiation
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; di-tert-butyl-diazodicarboxylate; cesium fluoride;
In
methanol; dichloromethane;
1: Mitsunobu reaction / 2: Suzuki coupling;
DOI:10.1021/co200062n
