Technology Process of C21H15Cl2NO2
There total 4 articles about C21H15Cl2NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Chloro-oxo-acetic acid; N,N-dimethyl-formamide;
In
dichloromethane;
for 1h;
Heating;
DOI:10.1021/jo026883p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / CuI; K2CO3; Cu / dibutyl ether / 120 h / 170 °C
2: NaOH / ethanol; H2O / 2 h / Heating
3: oxalylchloride; DMF / CH2Cl2 / 1 h / Heating
With
sodium hydroxide; copper(l) iodide; Chloro-oxo-acetic acid; copper; potassium carbonate; N,N-dimethyl-formamide;
In
ethanol; dichloromethane; dibutyl ether; water;
DOI:10.1021/jo026883p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / CuI; K2CO3; Cu / dibutyl ether / 120 h / 170 °C
2: NaOH / ethanol; H2O / 2 h / Heating
3: oxalylchloride; DMF / CH2Cl2 / 1 h / Heating
With
sodium hydroxide; copper(l) iodide; Chloro-oxo-acetic acid; copper; potassium carbonate; N,N-dimethyl-formamide;
In
ethanol; dichloromethane; dibutyl ether; water;
DOI:10.1021/jo026883p