3,7-Undecadienenitrile, 6-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-(1-ethoxyethoxy)-9-(1- methylethyl)-11-[[(4-methylphenyl)sulfonyl]oxy]-

Base Information

Chemical Name:3,7-Undecadienenitrile, 6-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-(1-ethoxyethoxy)-9-(1- methylethyl)-11-[[(4-methylphenyl)sulfonyl]oxy]-
CAS No.:103002-80-8
Molecular Formula:C42H57NO6SSi
Molecular Weight:732.069
Hs Code.:
Mol file:103002-80-8.mol

3,7-Undecadienenitrile,
6-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-(1-ethoxyethoxy)-9-(1-
methylethyl)-11-[[(4-methylphenyl)sulfonyl]oxy]-

Synonyms:

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Chemical Property of 3,7-Undecadienenitrile, 6-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-(1-ethoxyethoxy)-9-(1- methylethyl)-11-[[(4-methylphenyl)sulfonyl]oxy]-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,7-Undecadienenitrile, 6-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-(1-ethoxyethoxy)-9-(1- methylethyl)-11-[[(4-methylphenyl)sulfonyl]oxy]-

There total 6 articles about 3,7-Undecadienenitrile, 6-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-(1-ethoxyethoxy)-9-(1- methylethyl)-11-[[(4-methylphenyl)sulfonyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-6-Methyl-2-[4-(tetrahydro-furan-2-yloxy)-but-2-ynyl]-hept-4-ene-1,3-diol

: 103002-80-8
Toluene-4-sulfonic acid (4E,8Z)-(3R,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-10-cyano-10-(1-ethoxy-ethoxy)-3-isopropyl-deca-4,8-dienyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / Et₃N, DMAP

2: 2.) LiAlH₄

3: 1.) tosylation

4: H₂ / Pd-BaSO₄

With dmap; lithium aluminium tetrahydride; hydrogen; triethylamine; palladium on barium sulfate;
DOI:10.1021/jo00367a036

Reference yield:

: (E)-6-Methyl-3-oxo-2-[4-(tetrahydro-furan-2-yloxy)-but-2-ynyl]-hept-4-enoic acid methyl ester

: 103002-80-8
Toluene-4-sulfonic acid (4E,8Z)-(3R,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-10-cyano-10-(1-ethoxy-ethoxy)-3-isopropyl-deca-4,8-dienyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: LiAlH₄

2: 76 percent / Et₃N, DMAP

3: 2.) LiAlH₄

4: 1.) tosylation

5: H₂ / Pd-BaSO₄

With dmap; lithium aluminium tetrahydride; hydrogen; triethylamine; palladium on barium sulfate;
DOI:10.1021/jo00367a036

Reference yield:

: (E)-(5R,6S)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-10-(tetrahydro-furan-2-yloxy)-dec-3-en-8-yn-5-ol

: 103002-80-8
Toluene-4-sulfonic acid (4E,8Z)-(3R,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-10-cyano-10-(1-ethoxy-ethoxy)-3-isopropyl-deca-4,8-dienyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) LiAlH₄

2: 1.) tosylation

3: H₂ / Pd-BaSO₄

With lithium aluminium tetrahydride; hydrogen; palladium on barium sulfate;
DOI:10.1021/jo00367a036